bims-exposo Biomed News
on Exposomics
Issue of 2024‒11‒10
25 papers selected by
Yunjia Lai, Columbia University



  1. Ecotoxicol Environ Saf. 2024 Nov 01. pii: S0147-6513(24)01332-0. [Epub ahead of print]286 117256
      The increasing exposure to environmental chemicals calls for comprehensive non-targeted analysis to detect unrecognized substances in human samples. We examined human serum samples to classify compounds as endogenous or exogenous using public databases and to explore the relationships between exposure markers and metabolic patterns. Serum samples from 84 pregnant women at 32 weeks gestation were analyzed using LC-QToFMS. Using the PubChemLite for Exposomics database, we annotated and classified 106 compounds (51 endogenous, 55 exogenous). The compound patterns were analyzed using three dimensional reduction methods: Principal Component Analysis (PCA), regularized Generalized Canonical Correlation Analysis (rGCCA), and Uniform Manifold Approximation and Projection (UMAP). OPTICS clustering applied to these methods revealed two distinct clusters, with 89 % of significant compounds overlapping between clusters. The detected exogenous compounds included dietary substances, phthalates, nitrogenous compounds, and parabens. Pathway enrichment analysis showed that chemical exposure was linked to changes in amino acid metabolism, protein and mineral transport, and energy metabolism. While we found associations between exposure and metabolite changes, we could not establish causality. Our approach of analyzing both exogenous and endogenous chemicals from the same dataset using PubChemLite database presents a new method for exposome research, despite limitations in sample size and peak annotation accuracy. These findings contribute to understanding multiple chemical exposures and their metabolic effects in human biomonitoring.
    Keywords:  Clustering; Database; Liquid chromatography-high resolution mass spectrometry; Non-targeted analysis
    DOI:  https://doi.org/10.1016/j.ecoenv.2024.117256
  2. Stat Biosci. 2024 Jul;16(2): 482-502
      Environmental mixtures, which reflect joint exposure to multiple environmental agents, are a major focus of environmental health and risk assessment research. Advancements in latent variable modeling and psychometrics can be used to address contemporary questions in environmental mixtures research. In particular, latent variable models can quantify an individual's cumulative exposure burden to mixtures and identify hidden subpopulations with distinct exposure patterns. Here, we first provide a review of measurement approaches from the psychometrics field, including structural equation modeling and latent class/profile analysis, and discuss their prior environmental epidemiologic applications. Then, we discuss additional, underutilized opportunities to leverage the strengths of psychometric approaches. This includes using item response theory to create a common scale for comparing exposure burden scores across studies; facilitating data harmonization through the use of anchors. We also discuss studying fairness or appropriateness of measurement models to quantify exposure burden across diverse populations, through the use of mixture item response theory and through evaluation of measurement invariance and differential item functioning. Multi-dimensional models to quantify correlated exposure burden sub-scores, and methods to adjust for imprecision of chemical exposure data, are also discussed. We show that there is great potential to address pressing environmental epidemiology and exposure science questions using latent variable methods.
    Keywords:  Environmental epidemiology; Environmental health; Exposure mixtures; Item response theory; Latent variable models; Psychometrics
    DOI:  https://doi.org/10.1007/s12561-023-09410-9
  3. Front Public Health. 2024 ;12 1467121
      The key role of our microbiome in influencing our health status, and its relationship with our environment and lifestyle or health behaviors, have been shown in the last decades. Therefore, the human microbiome has the potential to act as a biomarker or indicator of health or exposure to health risks in the general population, if information on the microbiome can be collected in population-based health surveys or cohorts. It could then be associated with epidemiological participant data such as demographic, clinical or exposure profiles. However, to our knowledge, microbiome sampling has not yet been included as biological evidence of health or exposure to health risks in large population-based studies representative of the general population. In this mini-review, we first highlight some practical considerations for microbiome sampling and analysis that need to be considered in the context of a population study. We then present some examples of topics where the microbiome could be included as biological evidence in population-based health studies for the benefit of public health, and how this could be developed in the future. In doing so, we aim to highlight the benefits of having microbiome data available at the level of the general population, combined with epidemiological data from health surveys, and hence how microbiological data could be used in the future to assess human health. We also stress the challenges that remain to be overcome to allow the use of this microbiome data in order to improve proactive public health policies.
    Keywords:  biomarkers; cohort; metagenomics; microbiome; population; population-based health studies
    DOI:  https://doi.org/10.3389/fpubh.2024.1467121
  4. BMJ Open. 2024 Nov 01. 14(10): e087445
      INTRODUCTION: Air pollution presents a major public health threat to India, affecting more than three quarters of the country's population. In the current project, GEOHealth Health Effects of Selected Environmental Exposomes Across the Life CourSe-India, we aim to study the effect of environmental exposomes-fine particulate matter (PM2.5), nitrogen dioxide (NO2), ozone (O3) and extremes of temperature-on multiple health outcomes using a modified life course approach. The associated training grant aims to build capacity in India to address the unique environmental health problems.METHODS AND ANALYSIS: The project aims to (A) Develop exposure assessments in seven cities, namely Delhi, Chennai, Sonipat, Vizag, Pune, Hyderabad and Bikaner, for: (1) A fine-scale spatiotemporal model for multiple pollutants (PM2.5, NO2, O3, temperature); (2) Combined ground monitoring and modelling for major chemical species of ambient PM2.5 at seven cities; and (3) Personal exposure assessment in a subsample from the six cities, except Pune, and (B) Conduct health association studies covering a range of chronic non-communicable diseases and their risk factors leveraging a unique approach using interdigitating cohorts. We have assembled existing pregnancy, child, adolescent, adult and older adult cohorts across India to explore health effects of exposomes using causal analyses. We propose to use Bayesian kernel machine regression to assess the effects of mixtures of all pollutants including species of PM2.5 on health while accounting for potential non-linearities and interactions between exposures. This builds on earlier work that constructed a fine spatiotemporal model for PM2.5 exposure to study health outcomes in two Indian cities.
    ETHICS AND DISSEMINATION: Ethical clearance for conduct of the study was obtained from the Institutional Ethics Committee (IEC) of the Centre for Chronic Disease Control, and all the participating institutes and organisations. National-level permission was provided by the Indian Council of Medical Research. The research findings will be disseminated through peer-reviewed publications, policy briefs, print and social media, and communicating with the participating communities and stakeholders. Training of Indian scientists will build the capacity to undertake research on selected adverse environmental exposures on population health in India.
    Keywords:  epidemiologic studies; epidemiology; public health
    DOI:  https://doi.org/10.1136/bmjopen-2024-087445
  5. Sci Rep. 2024 11 02. 14(1): 26375
      In recent years, worldwide fertility rates have continued to decrease. Humans are frequently exposed to a combination of environmental endocrine disruptors, which can cause male reproductive disorders. The study employed three distinct analytical models to examine the correlation between exposure to a combination of 25 chemicals and sex steroid hormone levels in adult males. This involved evaluating 12 chemicals and their metabolites from personal care and consumer products, as well as 13 metabolites linked to phthalates and plasticisers. The study analysed 25 chemicals and 3 measured sex steroid hormone outcomes, as well as two calculated hormonal outcomes (free androgen index, TT/E2 ratio) in 1262 adult men who participated in the National Health and Nutrition Examination Survey (NHANES) 2013-2016 in the United States. The study employed several statistical methods to estimate the relationships between single chemicals or chemical blends and sex hormones. These methods included linear regression, weighted quantile sum (WQS) regression, and Bayesian kernel machine (BKMR) regression. The results of the linear regression analysis indicate that chemical exposure has a negative correlation with E2, TT, and FAI, and a positive correlation with SHBG and TT/E2. The mixture effect analyses using the WQS and BKMR models further confirmed that BP3, MECPP, and MECOP were the most highly weighted chemical mixtures. The analyses also suggested that there were differences in the effects of different concentrations of EDCs on sex steroid hormones. Exposure to environmental endocrine-disrupting chemicals (EDCs) has been found to have a negative correlation with estradiol and total testosterone, as well as FAI. Conversely, this exposure has been found to have a positive correlation with sex hormone binding globulin and the TT/E2 ratio. The study also revealed differences in the effects of different concentrations of EDCs.
    Keywords:  Environmental endocrine disrupting chemicals (EDCs); NHANES; Sex steroid hormones
    DOI:  https://doi.org/10.1038/s41598-024-76972-z
  6. Environ Health Insights. 2024 ;18 11786302241296225
      Despite growing attention and guiding frameworks, we still know very little about how environmental exposures may be contributing to the health inequities experienced by sexual and gender minority (SGM) people, especially exposures beyond psycho-behavioral mechanisms that have traditionally been viewed as the pathways between minority stress and negative health outcomes. To address this gap in knowledge, we conducted a scoping review to determine the extent to which disparities in environmental exposures between SGM and non-SGM (ie, heterosexual and cisgender) populations have been measured in the United States. We searched PubMed for studies that were (1) peer-reviewed; (2) written in English; (3) quantitatively measured environmental exposures; (4) included 1 or more groups identifying as a sexual minority, gender minority, or both; (5) compared to the general population; (6) in the United States; and (7) published on or after January 1, 2011. Our scoping review identified very few studies that examined and documented environmental exposure disparities between SGM and non-SGM populations in the United States. These studies focused mostly on cigarette smoke exposures. None examined environmental exposure disparities between gender minority and cisgender populations. To address this critical gap in environmental health research for SGM populations in the short term, researchers can merge existing environmental data (eg, data from the Environmental Protection Agency) with SGM population data. Longer-term solutions require systematically including validated sexual orientation and gender identity measures across federal, state, and local datasets, as well as increased funding for original research that explores diverse environmental exposures. Taken together, these efforts can significantly advance our ability to identify and address environmental health inequities experienced by SGM people.
    Keywords:  LGBT; SGM; Sexual minority; gender minority; scoping review
    DOI:  https://doi.org/10.1177/11786302241296225
  7. Ecotoxicol Environ Saf. 2024 Nov 01. pii: S0147-6513(24)01312-5. [Epub ahead of print]286 117236
      Bisphenol A (BPA) is an environmental contaminant and can be detected in foodstuffs. Hence, investigating BPA metabolism in humans is crucial because certain BPA metabolites may exhibit similar or even greater be toxicity than does the parent compound. In this study, we used an advanced metabolomics-based data processing approach along with ultraperformance liquid chromatography-mass spectrometry (UPLC-MS) to identify BPA metabolites in human liver enzyme incubation samples, and those metabolites were further detected in human excreta and water body samples in Taiwan. The first stage involved converting full-scan MS files from the incubation samples into feature information; this stage revealed 1056 and 2472 features with dose-response relationships in the BPA and isotopically labeled BPA incubation datasets, respectively. The second stage involved using stable isotope tracing to identify isotopic pairs from the two datasets; this stage revealed 190 isotopic pairs. An additional dose-response experiment was conducted to confirm that all these features with isotopic pairs also exhibited a dose-response relationship. To focus on the primary BPA metabolite features, we excluded those with low intensities (below 50,000). This left us with 86 features, which we then used for our analysis. To confirm these features as possible BPA metabolites, we compared the tandem MS (MS/MS) spectra between BPA and isotopically labeled BPA incubation samples. The results revealed 75 isotopic pairs with matching isotopically labeled MS/MS spectra. Among these identified features, one feature's m/z value matched to that of a previously reported BPA metabolite, and the other 74 features were novel. However, only 9 of them had proposed structures. We further investigated whether these features could be detected in humans or Taiwanese water bodies. Furthermore, 10 and 2 novel metabolites were identified in human urine and fecal samples, respectively; 17 novel metabolites were identified in the water samples. These findings indicate some of these novel metabolites are present not only in humans but also in various water bodies across Taiwan. These identified metabolites are phase I BPA metabolites, suggesting they may have toxic properties. Further research is warranted to investigate the structures of these newly discovered metabolites and assess their potential human health risks.
    Keywords:  Bisphenol A; Dose–response technique; High-resolution mass spectrometry; Metabolomics-based data processing approach; Taiwanese water bodies
    DOI:  https://doi.org/10.1016/j.ecoenv.2024.117236
  8. J Chromatogr A. 2024 Nov 22. pii: S0021-9673(24)00825-2. [Epub ahead of print]1737 465451
      High efficiency in the analytical workflow, including fast sample preparation and LC-MS/MS analysis, is an advantage when analyzing a high number of samples. It can however be a challenge when determining polar analytes in complex, biological samples, and one must expect to make a compromise between a simple sample preparation followed by a long chromatographic separation, or vice versa, to limit matrix effects. In this proof-of-concept work, a one-step 96-well (parallel extraction) electromembrane extraction (EME) method was coupled to flow injection-MS/MS of 0.7 min per sample, allowing a very high-throughput analysis of 12 polar, endogenous metabolites from unprecipitated plasma of limited dilution. The throughput of the EME method matched the subsequent analysis. Recoveries ranged from 6 to 93 %, and repeatability and linearity were 2-15 % and R2 ≥ 0.9949, respectively, for all but two compounds. Matrix effects were approximately 50 % after EME and varied <11 % between 6 plasma donors, which represented a major improvement relative to a simple protein precipitation where signals were entirely suppressed. The work demonstrates a potential for EME coupled to flow injection-MS/MS to serve as a high-throughput platform for bioanalysis, not just of polar analytes, but also hydrophobic drugs both basic and acidic.
    Keywords:  Acetyl choline; Electromembrane extraction; Flow injection - mass spectrometry; High throughput; Polar endogenous metabolites
    DOI:  https://doi.org/10.1016/j.chroma.2024.465451
  9. Environ Int. 2024 Oct 20. pii: S0160-4120(24)00675-5. [Epub ahead of print]193 109089
      Growing concerns about the environmental impact of ionic liquids (ILs) have spurred research into their (eco)toxic effects, but studies on their mode of toxic action (MOA) still remain limited. However, understanding the MOA and identifying structural features responsible for enhanced toxicity is crucial for characterising the hazard and designing safer alternatives. Therefore, 45 ILs, with systematically varied chemical structures, were tested for cytotoxicity and two specific endpoints in reporter gene assays targeting the Nrf2-ARE mediated oxidative stress response (AREc32) and aryl hydrocarbon receptor activation (AhR-CALUX). While none of the ILs activated the reporter genes, cytotoxicity was high and markedly different between cell lines. Seven and 25 ILs proved more cytotoxic than predicted by baseline toxicity model in the AREc32 and the AhR-CALUX assays, respectively. The length of the side chain and headgroup structures of ILs altered the MOA of ILs. Cellular metabolism of the ILs, investigated by LC-MS/MS, showed side-chain oxidation of the long-chain quaternary ammonium compounds in AhR-CALUX cells and, to a lower extent, in AREc32 cells, however, this transformation could not explain the high cytotoxicity. Effect data for 72 ILs for ten endpoints retrieved from the Tox21 database identified the inhibition of aromatase activity and of mitochondrial membrane potential as potential MOAs. However, in vitro fluorimetric assays for these endpoints demonstrated that effects were activated in a non-specific manner, probably through cytotoxicity. Although many of the ILs tested induced cytotoxicity at concentrations lower than baseline toxicity, the specific MOAs responsible could not be identified. Alternatively, we suggest that the descriptors currently used may fail to define the affinity of ILs for cells. Testing of the affinity of ILs for a diverse range of biomolecules is needed to accurately describe their interactions with cells.
    Keywords:  Baseline toxicity; Cytotoxicity; Ionic liquids; Membrane-water partitoning; Mode of toxic action; Structure–activity relationships
    DOI:  https://doi.org/10.1016/j.envint.2024.109089
  10. Heliyon. 2024 Oct 30. 10(20): e39490
      The interest in characterization of drugs abused started in 1948 with the aim of determining the origin of opium. After 75 years there is still a great interest in this approach, called geo-profiling, chemical or forensic profiling in the following decades. Recently chemical attribution signatures (CAS) were proposed by the authors who studied "synthesis precursors and byproducts, impurities, degradation products, and metabolites in various biological matrices" of fentanyl. Forensic profiling evolved during these decades: new analytical approaches were tested and it was applied to more and more products, which threaten the health and security of citizens worldwide. In substances of natural origins (e.g. opium, cannabis and cocaine), it is possible to exploit the great variability of both elements and organic chemical compounds and to study chemical compounds such as reagents and solvents, by-products, and cutting agents used in the production chain. Profiles can be used to classify products from different seizures into groups of similar samples (tactical intelligence) or to determine the origin of samples (strategic intelligence). Chromatographic approaches coupled to mass spectrometry are very common to determine organic profiles, while elemental profiles are obtained by nuclear activation analysis, inductively coupled plasma mass spectrometry or ion beam analysis. A very important role in the field is played by isotope ratio analysis. Approaches to obtain forensic profiles are available also for chemical warfare agents, explosives, illegal medicines, doping agents, supplements, food. Chemometrics can be particularly useful to establish the authenticity of products and for the interpretation of large amount of forensic data. The future of forensic profiling is a challenge for forensic sciences. Organized crime is involved in the manufacturing of a large number of illegal products and forensic profiling is a very powerful tool to support the health of citizens and the administration of justice worldwide.
    Keywords:  Chemical attribution signatures (CAS); Chemical profiling; Chemical warfare agents; Counterfeit medicines; Doping agents; Geo-profiling; Illicit drugs
    DOI:  https://doi.org/10.1016/j.heliyon.2024.e39490
  11. Environ Res. 2024 Oct 30. pii: S0013-9351(24)02160-1. [Epub ahead of print]263(Pt 3): 120253
      BACKGROUND: Environmental chemical exposures in utero may play a role in autism development. While preconception risk factors for autism are increasingly being investigated, little is known about the influence of chemical exposures during the preconception period, particularly for paternal exposures.METHODS: In 195 children from the Preconception Environmental exposures And Childhood health Effects (PEACE) cohort born to parents recruited from a fertility clinic in Boston, Massachusetts between 2004 and 2017, we quantified concentrations of 11 phthalate metabolites and bisphenol A (BPA) in urine samples collected from mothers and fathers before conception and mothers throughout pregnancy. When children were 6-15 years old, parents completed the Social Responsiveness Scale (SRS) questionnaire assessing autistic behaviors. We used linear mixed effect models to estimate covariate-adjusted associations of phthalate biomarker and BPA concentrations, separately for maternal preconception (n = 179), paternal preconception (n = 121), and maternal pregnancy (n = 177), with SRS T-scores, based on age and gender, in offspring. We used quantile g-computation models for mixture analyses and evaluated modification by selected dietary factors.
    RESULTS: The mean SRS T-score was 47.7 (±7.4), lower than the normative mean of 50. In adjusted models for individual biomarkers or mixtures, few associations were observed and estimates were generally negative (e.g., lower SRS T-scores) and imprecise. We observed associations of higher mono-isobutyl phthalate (MiBP) concentrations measured in maternal preconception and paternal preconception periods with lower SRS T-scores (βmaternal_precon = -1.6, 95% CI -2.7; -0.4; βpaternal_precon = -2.9, 95% CI -4.6; -1.2) for each loge increase. In a subset of participants with maternal preconception nutrition information, we generally observed stronger inverse associations with higher folate and iron intake, particularly for folate intake and MiBP concentrations.
    CONCLUSIONS: Urinary phthalate biomarker and BPA concentrations during preconception (maternal and paternal) and pregnancy (maternal) were not associated with adverse autistic behaviors in these children. Larger studies are needed to elucidate the observed associations, while considering interactions between maternal nutrition and chemical exposures.
    Keywords:  Autism; Bisphenol A; Endocrine disrupting chemicals; Offspring health; Phthalates; Preconception; Pregnancy
    DOI:  https://doi.org/10.1016/j.envres.2024.120253
  12. Int J Biol Sci. 2024 ;20(14): 5779-5792
      The escalation of plastic pollution represents a global environmental and health problem. Important toxic effects have been attributed to the increasing diffusion of microplastics (MPs) and nanoplastics (NPs) derived from the degradation of plastics. These particles have been ubiquitously observed in the environment, with humans being continuously exposed via ingestion, inhalation and skin contact. Nonetheless, the cellular homeostasis imbalance induced by micro- and nano- plastics (MNPs) in human health has been only recently shown, while most evidence and molecular mechanisms derived from studies in vitro and in vivo models. To date, the majority of available results testified the accumulation of MNPs in the cardiovascular, nervous, reproductive and digestive systems, and recently clear evidence about cardiovascular toxic effects of MNPs has been provided in humans. In this context, this review aims to provide a comprehensive update about the most recent studies reporting the effects of MNPs in different models, focusing on the available evidence in the main areas of study related to human health. Hopefully, this review will contribute to raise awareness about the toxicity and oxidative alteration exerted by MNPs, supporting the elaboration of new strategies to counteract plastic pandemics.
    Keywords:  human health threat; microplastics; nanoplastics; oxidative stress; toxic effects
    DOI:  https://doi.org/10.7150/ijbs.99556
  13. J Chem Inf Model. 2024 Nov 03.
      The increasing need to understand and control the environmental impact of chemical processes has revealed the challenge in efficient evaluation of toxicity of the vast number of chemical compounds and their varying effects on biological systems. In this study, we introduce "Build-a-bio-Strip", a novel online service designed to carry out a quick initial analysis of the toxic impact of chemical processes. This platform enables users to automatically generate toxicity characteristics of chemical reactions using their own data on cytotoxicity or median lethal doses of the substances involved or computational predictions based on SMILES strings. The service calculates the toxicity metrics such as bio-Factors and cytotoxicity potentials, which can be used to identify the substances with significant contributions to the overall toxicity of a particular process. This facilitates the selection of safer synthetic routes and the optimization of chemical processes from a toxicity perspective. "Build-a-bio-Strip" represents a step toward safer and more sustainable chemical practices. It is available free-of-charge at http://app.ananikovlab.ai:8080/.
    DOI:  https://doi.org/10.1021/acs.jcim.4c01381
  14. Community Sci. 2024 Sep;pii: e2024CSJ000088. [Epub ahead of print]3(3):
    Knights Landing Promotoras
      Environmental justice research driven by academics and policymakers often overlooks the valuable insights and leadership of the communities most impacted by environmental hazards. When institution-led research approaches are employed, inadequate community ownership and limited institutional accountability hinder the effectiveness of environmental public health interventions. In contrast, a community-owned and -managed approach to environmental justice research can guide community members in developing evidence-based interventions. This paper outlines a community-led environmental health assessment survey (sample= 100) and resulting community actions over six years (2017 to 2023) in a Northern California farmworker community with a perceived high prevalence of cancer and exposure to environmental hazards in households, neighborhoods, and job sites. Local resident experts in Knights Landing, CA, documented community risk factors and exposures in collaboration with interdisciplinary undergraduate and graduate student-researchers. The survey instrument focused on environmental hazards identified by local resident experts including vehicular and agricultural pollution, occupational pesticide contact, and sun exposure. Survey findings highlighted the need for targeted interventions to reduce environmental health risks, such as academic outreach programs, county investments in public services, and community-led mutual aid initiatives. Despite academic reservations about our non-random sampling method and data collection by local resident experts, our project sparked substantial actions and investments with minimal personnel and financial resources. Local leaders working with student-researchers developed more effective environmental public health interventions through a community-owned and -managed approach that went beyond the efforts of local regulatory and research institutions.
    Keywords:  Environmental justice; agricultural; carcinogen; community health assessment survey; community-based participatory action research; rural
    DOI:  https://doi.org/10.1029/2024csj000088
  15. Microb Cell Fact. 2024 Nov 05. 23(1): 298
      Zeaxanthin, a vital dietary carotenoid, is naturally synthesized by plants, microalgae, and certain microorganisms. Large-scale zeaxanthin production can be achieved through plant extraction, chemical synthesis, or microbial fermentation. The environmental and health implications of the first two methods have made microbial fermentation an appealing alternative for natural zeaxanthin production despite the challenges in scaling up the bioprocess. An intermediate between β-carotene and zeaxanthin, β-cryptoxanthin, is found only in specific fruits and vegetables and has several important functions for human health. The low concentration of β-cryptoxanthin in these sources results in low extraction yields, making biotechnological production a promising alternative for achieving higher yields. Currently, there is no industrially relevant microbial fermentation process for β-cryptoxanthin production, primarily due to the lack of identified enzymes that specifically convert β-carotene to β-cryptoxanthin without further conversion to zeaxanthin. In this study, we used genetic engineering to leverage the oleaginous yeast Yarrowia lipolytica as a bio-factory for zeaxanthin and β-cryptoxanthin production. We screened 22 β-carotene hydroxylases and identified eight novel enzymes with β-carotene hydroxylating activity: six producing zeaxanthin and two producing only β-cryptoxanthin. By introducing the β-carotene hydroxylase from the bacterium Chondromyces crocatus (CcBCH), a β-cryptoxanthin titer of 24 ± 6 mg/L was achieved, representing the highest reported titer of sole β-cryptoxanthin in Y. lipolytica to date. By targeting zeaxanthin-producing β-carotene hydroxylase to the endoplasmic reticulum and peroxisomes, we increased the production of zeaxanthin by 54% and 66%, respectively, compared to untargeted enzyme. The highest zeaxanthin titer of 412 ± 34 mg/L was achieved by targeting β-carotene hydroxylases to peroxisomes. In addition, by constructing multienzyme scaffold-free complexes with short peptide tags RIDD and RIAD, we observed a 39% increase in the zeaxanthin titer and a 28% increase in the conversion rate compared to the strain expressing unmodified enzyme. The zeaxanthin titers obtained in this study are not the highest reported; however, our goal was to demonstrate that specific approaches can enhance both titer and conversion rate, rather than to achieve the maximum titer. These findings underscore the potential of Y. lipolytica as a promising platform for carotenoid production and provide a foundation for future research, where further optimization is required to maximize production.
    Keywords:   Yarrowia lipolytica ; Carotenoids; Metabolic engineering; Modular enzyme assembly; Multienzyme complex; Subcellular compartments; Zeaxanthin; β-cryptoxanthin
    DOI:  https://doi.org/10.1186/s12934-024-02569-w
  16. Glob Health Epidemiol Genom. 2024 ;2024 6103589
      This research presents a time-series study in one of the most polluted regions in Mexico, the southern part of the Mezquital Valley. Three mortality causes related to areas highly contaminated by industrial activities were considered to carry out this model, namely, ischemic cardiomyopathy, mesothelioma, and pneumoconiosis. The pollutant exposure factors used in the maximum entropy modeling were distance to rivers, distance to industries, particulate matter less than 2.5 microns (PM < 2.5 µm), and the digital elevation model (DEM). A model that expresses the presence of the disease by areas of exposure to pollutants was also obtained. In addition, the odds ratio was calculated to evaluate the level of association of ischemic cardiomyopathy (OR = 3.37 and 95% CI: 3.05-3.6) and mesothelioma (OR = 4.79 and 95% CI: 3.5-6.08) by areas of exposure. In the case of pneumoconiosis, only cases in the very high exposure category were recorded, so it was not comparable with the remaining areas. It is important to mention that particulate matter in the municipalities of the Mezquital Valley presented values above 20 μg/m3 and that in accordance with the provisions of the Norma Oficial Mexicana de Salud Ambiental or NOM (translated as Mexican Official Standard for Environmental Health) and the Agency for Toxic Substances and the Disease Registry (ATSDR), high concentrations of particulate matter can have a severe impact on the development of some diseases. In the studied area, ischemic cardiomyopathy and mesothelioma were attributed to pollution in 70.3% and 79.1%, respectively; therefore, pollution mitigation could prevent the occurrence of these two diseases.
    DOI:  https://doi.org/10.1155/2024/6103589
  17. Transl Gastroenterol Hepatol. 2024 ;9 75
      Background and Objective: Complementary and integrative health (CIH) approaches are increasingly popular among patients with gastrointestinal (GI) disorders. Whole person health has been identified as an important perspective in integrative health. While complementary approaches have been discussed in the GI literature, the whole person health framework has not yet been incorporated. Whole person health is particularly relevant as we shift to patient-centered care to facilitate holistic healing for this population. The aim of this paper is to apply a conceptualization of whole person health and its relevance in understanding how CIH approaches can be utilized for patients with stress-sensitive GI disorders, such as disorders of gut-brain interaction (DGBI) and inflammatory bowel disease (IBD).Methods: Between July 2023 and December 2023 numerous major databases were reviewed to identify relevant articles for this narrative review. Keywords searched included (but not limited to) complementary alternative medicine, integrative medicine, DGBI, IBD, whole person health, and CIH categories (nutritional, mind-body, psychological). We limited our search to peer-reviewed English language articles. Studies were also cross-referenced to incorporate additional relevant studies.
    Key Content and Findings: This narrative review describes how to integrate CIH approaches with whole person health for patients with some of the most common stress-sensitive GI disorders, including DGBIs and IBD. In each section, we highlight how each domain of the whole person health framework (biological, behavioral, social, environmental) can be addressed through CIH approaches: psychological, mind-body practices, and nutritional.
    Conclusions: The integration of CIH approaches into the treatment of GI disorders is a growing area of interest that holds promise for enhancing patient outcomes. The two concepts of CIH and whole person health are harmonizing, and their integration serves to support patients who are already using CIH approaches, and providers who can facilitate shared-decision-making and patient-centered care. While not exhaustive, this review demonstrates positive associations between the use of CIH and beneficial outcomes across all whole person health domains for patients with GI disorders.
    Keywords:  Complementary and integrative health (CIH); complementary and alternative health; disorders of gut-brain interaction (DGBI); inflammatory bowel disorder; whole person health
    DOI:  https://doi.org/10.21037/tgh-23-121
  18. Environ Res. 2023 Oct 28. pii: S0013-9351(23)02310-1. [Epub ahead of print] 117506
      Exposure to low doses of neonicotinoid (NEO) insecticides during pregnancy may have a negative impact on the neurodevelopment of children. Biomarkers are frequently used to investigate the exposure and its health effects in environmental epidemiology. In the present study, we aimed to evaluate the utility of urinary biomarkers of NEO exposure by calculating intra-class correlation coefficients (ICCs). Urine samples were collected from 30 pregnant women who were non-smokers and living in a central part of Japan, between 12 and 22 weeks of gestation. We collected first morning voided (FMV) urine and afternoon spot (PM) urine samples on the same day on five occasions within a 2-week period. The urinary concentrations of NEO and their metabolites (NEO/m) were measured by liquid chromatography-tandem mass spectrometry. Normalisation to the specific gravity and creatinine concentration was used in the calculation of ICC. The number of urine samples required to obtain a reliable biomarker estimate of NEO exposure was calculated. The most frequently detected NEO/m was N-desmethyl-acetamiprid (N-dm-ACE), followed by clothianidin (CLO), thiamethoxam (THX) and dinotefuran (DIN), in both FMV and PM urine samples. The ICC calculations showed poor reproducibility for the measurement of CLO and THX concentrations (ICCs ≤0.25) in both FMV and PM urine samples and for DIN (ICC ≤0.29) in the FMV urine samples, and moderate reproducibility was identified for N-dm-ACE (ICC >0.60) in both FMV and PM urine samples and for DIN (ICC >0.40) in the PM urine samples. A minimum of 1-19 spot urine samples per individual was required to provide a reliable biomarker estimate over a 2 week period. These results suggest that pregnant Japanese women are frequently exposed to NEOs, and that, with the exception of urinary N-dm-ACE, a single measurement of urinary NEO concentrations may not be an appropriate method of characterising overall exposure.
    Keywords:  Biomarker; Human exposure; Intra-class correlation coefficient; Metabolite; Neonicotinoid; Pregnant woman
    DOI:  https://doi.org/10.1016/j.envres.2023.117506
  19. Sci Total Environ. 2024 Oct 26. pii: S0048-9697(24)07301-7. [Epub ahead of print] 177144
      Exposure to chemical mixtures is the norm in natural environments. Yet, water quality regulations are still mostly constructed for individual chemicals. However, an important ambition of the European Green Deal is the future implementation of mixture toxicity to address the risks posed by the joint presence of multiple chemicals in aquatic ecosystems (e.g., via a mixture allocation factor, MAF). This study aimed to contribute to this by investigating the ecotoxicity of a series of binary ciprofloxacin‑copper (CIP-Cu) mixtures at environmental realistic concentrations to the cyanobacterium Microcystis aeruginosa, which is the most CIP-sensitive freshwater species identified so far. The two chemicals have distinct modes of action, however, the bioavailability of both is influenced by pH. The toxicity data of CIP-Cu mixtures were analysed to examine if significant interactions exist relative to the concentration addition (CA) and independent action (IA) models. CIP-Cu mixtures behaved antagonistically relative to the CA model, whereas there was no interactive toxicity relative to the IA model, which better describes the CIP-Cu mixture toxicity, in line with expectations based on the distinct modes of action of Cu and CIP. Furthermore, attention was placed to the influence of Cu in the low-effect concentration range (≤ EC10, the 10 % effective concentration) on CIP ecotoxicity, in order to identify potential synergistic effects that may lower the toxic threshold of CIP in the presence of Cu. Across the pH range 7.3-9.0, the presence of '≤ EC10' level of Cu did not affect the EC10 of CIP. Only at pH 8.0, but not at pH 7.3 or 9.0, the addition of an (EC10)/2 level of Cu lowered the 50 % effect concentration (EC50) of CIP from 2.8 to 2.0 μg L-1. The overall observations confirmed that there are no significant interactive effects between Cu and CIP relative to the IA model. Therefore, regulatory environmental threshold concentrations for CIP derived from single-chemical tests, are protective in situations of co-occurrence with Cu, provided that Cu remains below its own environmental quality standards.
    DOI:  https://doi.org/10.1016/j.scitotenv.2024.177144
  20. Data Brief. 2024 Dec;57 111021
      This article presents a dataset on 71 pesticide levels and the identification of additional synthetic organic chemicals, including pharmaceuticals and industrial compounds, in L'Albufera Natural Park (Valencia, Spain). Sampling was conducted during May-June (spring) and end of September-October (autumn) 2019, timed to the rice cultivation cycle, the region's main agricultural activity. A total of 130 samples (100 water and 30 sediments) were collected from 51 strategically selected sites, including rivers, irrigation channels, Albufera Lake, and Mediterranean outlets, utilizing a combination of targeted and non-targeted screening (NTS) methods. The dataset encompasses physical-chemical parameters for both spring and autumn seasons. Advanced analytical techniques, such as high-resolution mass spectrometry (HRMS), were employed to detect contaminants beyond traditional methods, providing critical insights for environmental management and policy development. The findings contribute to addressing gaps in knowledge regarding contaminants of emerging concern (CECs) and their distribution across different environmental compartments. These data supplement the findings of the research article "Fingerprinting of Emerging Contaminants in L'Albufera Natural Park (Valencia, Spain): Implications for Wetland Ecosystem Health".
    Keywords:  Industrial compounds; Pesticides; Pharmaceuticals; Sediments; Spatial distribution; Surface waters
    DOI:  https://doi.org/10.1016/j.dib.2024.111021
  21. Endocrinology. 2024 Nov 05. pii: bqae149. [Epub ahead of print]
      Surfactants are molecules with both hydrophobic and hydrophilic structural groups that adsorb at the air-water or oil-water interface and serve to decrease the surface tension. Surfactants combine to form micelles that surround and break down or remove oils, making them ideal for detergents and cleaners. Two of the most important classes of nonionic surfactants are alkylphenol ethoxylates (APEOs) and alcohol ethoxylates (AEOs). APEOs and AEOs are high production-volume chemicals that are used for many industrial and residential purposes, including laundry detergents, hard-surface cleaners, paints, and pesticide adjuvants. Commensurate with better appreciation of the toxicity of APEOs and the base alkylphenols, use of AEOs has increased, and both sets of compounds are now ubiquitous environmental contaminants. We recently demonstrated that diverse APEOs and AEOs induce triglyceride accumulation and/or pre-adipocyte proliferation in vitro. Both sets of contaminants have also been demonstrated as obesogenic and metabolism disrupting in a developmental exposure zebrafish model. While these metabolic health effects are consistent across models and species, the mechanisms underlying these effects are less clear. This study sought to evaluate causal mechanisms through reporter gene assay assessments, relative binding affinity assays, co-exposure experiments, and use of both human cell and zebrafish models. We report that antagonism of thyroid hormone receptor signaling appears to mediate at least a portion of the polyethoxylate-induced metabolic health effects. These results suggest further evaluation is needed, given the ubiquitous environmental presence of these thyroid disrupting contaminants and reproducible effects in human cell models and vertebrate animals.
    Keywords:  Adipogenesis; Alcohol ethoxylates; Alkylphenol ethoxylates; Endocrine Disrupting Chemicals; Ethoxylated Surfactants; Mixtures
    DOI:  https://doi.org/10.1210/endocr/bqae149
  22. J Hazard Mater. 2024 Oct 28. pii: S0304-3894(24)02895-4. [Epub ahead of print]480 136316
      Release of persistent and potentially toxic per- and polyfluoroalkyl substances (PFAS) and other halogenated compounds into the aqueous environment is an emerging issue and advanced treatment methods are needed for their removal from contaminated water. Destructive treatment methods for PFAS exist, but there is a risk of incomplete degradation, resulting in creation of transformation products during treatment. This study assessed the potential of electrochemical oxidation (EO) for destruction of PFAS and other halogenated compounds, and their transformation products. Suspect and non-target screening were used to explore the chemical space of these samples and identify compounds present before and after the treatment, including transformation products. In total, 21 PFAS classes and 53 individual PFAS were identified using suspect and non-target screening, with confidence level (CL) 3d or higher. Two new classes of PFAS (FASHN and MeOH-FASA) were discovered for the first time. Suspect screening of PFAS revealed that hydro-substituted and ether PFAS could be formed during EO. A total of 12 chlorinated and two brominated compounds were also detected and confirmed with CL 1-3, with six compounds determined to be transformation products. Formation of ammonium oxidation byproducts was hypothesized as being responsible for most identified transformation products formed during EO.
    Keywords:  Destructive treatment; Electrochemical oxidation; High-resolution mass spectrometry; Non-target screening; Per- and polyfluoroalkyl substances; Transformation products
    DOI:  https://doi.org/10.1016/j.jhazmat.2024.136316
  23. J Chromatogr A. 2024 Oct 29. pii: S0021-9673(24)00858-6. [Epub ahead of print]1738 465484
      We developed a novel approach to selectively isolate or remove nearly any compound from complex mixtures of volatile organic compounds. This was achieved by customizing a GC×GC system with a Deans switch, a passive splitter, and a custom-made adapter for sample recollection. The new setup was evaluated with 106 standard chemicals covering a wide range of volatility (boiling points: 56 - 343 ⁰C) and polarity (log P: 0.2 - 9.4). The method was used to remove two notorious malodorous compounds from spoiled wine samples. We found that the recovery can be maximized if a custom-made adapter is attached directly on the flame ionization detector port (average recovery rate of 76 ± 7 % for the standards). Eventually, we could selectively isolate or remove chemicals with peaks separated by a minimum distance of 50 ms for the second column throughout the whole chromatographic run. The developed system is expected to mainly be used in the field of flavor and fragrance analysis (i.e., selection of flavors and odorants of interest or removal of off-flavor or malodorous compounds). At present, we can reasonably collect about 100 ng of each single compound and are currently working on sample enrichment to improve our method to isolate sufficient amounts for further chemical analysis (e.g. high sensitivity nuclear magnetic resonance or chemical ionization tandem mass spectrometry).
    Keywords:  Chemical isolation; Comprehensive two-dimensional GC; Flavor and fragrances; Preparative GC; Thermal desorption; Volatile organic compounds
    DOI:  https://doi.org/10.1016/j.chroma.2024.465484
  24. Sci Total Environ. 2024 Nov 04. pii: S0048-9697(24)07548-X. [Epub ahead of print] 177391
      Airborne pollutants like particulate matter and volatile organic compounds can negatively impact microbial, plant, and animal life as well as human health. Traditional environmental monitoring, while crucial, often relies on expensive equipment at limited locations, leading to gaps in geographical coverage. To obtain a low-cost, easily deployed environmental monitoring grid, the use of European honey bees (Apis mellifera) as biomonitor can offer a promising alternative. Their extensive foraging in the landscape exposes them to environmental contaminants like particulate matter and organic compounds. Once collected, these pollutants are carried back into the hives, where they can subsequently be sampled and quantified using various techniques. This potentially makes honey bee colonies a cost-effective and valuable long-term monitoring tool for particulate matter and organic compounds. This review, through the critical insight of the most recent pertinent literature, explores the suitability of honey bees and their products as biomarkers for environmental monitoring of these pollutants, addressing sample preparation approaches and chemical analytical methods. Overall, the presented information will aid researchers in initiating further investigations in this pivotal field, incorporating additional chemicals and innovative, non-invasive sampling matrices compatible with the beehive environment.
    Keywords:  Environmental monitoring; Honey bees; Particulate matter; Passive sampling; Volatile organic compounds
    DOI:  https://doi.org/10.1016/j.scitotenv.2024.177391
  25. Microplast nanoplast. 2024 ;4(1): 25
      While tire wear particles (TWP) have been estimated to represent more than 90% of the total microplastic (MP) emitted in European countries and may have environmental health effects, only few data about TWP concentrations and characteristics are available today. The lack of data stems from the fact that no standardized, cost efficient or accessible extraction and identification method is available yet. We present a method allowing the extraction of TWP from soil, performing analysis with a conventional optical microscope and a machine learning approach to identify TWP in soil based on their colour. The lowest size of TWP which could be measured reliably with an acceptable recovery using our experimental set-up was 35 µm. Further improvements would be possible given more advanced technical infrastructure (higher optical magnification and image quality). Our method showed a mean recovery of 85% in the 35-2000 µm particle size range and no blank contamination. We tested for possible interference from charcoal (as another black soil component with similar properties) in the soils and found a reduction of the interference from charcoal by 92% during extraction. We applied our method to a highway adjacent soil at 1 m, 2 m, 5 m, and 10 m and detected TWP in all samples with a tendency to higher concentrations at 1 m and 2 m from the road compared to 10 m from the road. The observed TWP concentrations were in the same order of magnitude as what was previously reported in literature in highway adjacent soils. These results demonstrate the potential of the method to provide quantitative data on the occurrence and characteristics of TWP in the environment. The method can be easily implemented in many labs, and help to address our knowledge gap regarding TWP concentrations in soils.Supplementary Information: The online version contains supplementary material available at 10.1186/s43591-024-00102-9.
    Keywords:  Machine learning; Microplastic; Optical microscopy; Segmentation; Soil pollution; Tire wear
    DOI:  https://doi.org/10.1186/s43591-024-00102-9